Oxygen,Nitrogen,andHydrogeninRefractoryMetalsSummaryOneofthemostcriticalchemicalspecificationsoftitaniumalloysisthehydrogencontent.Toohighofahydrogencontentcancausehydridestoprecipitate,whichcanleadtoembrittlementandsubsequentcrackingwhenthealloyisstressed.Hydrogenpickuptypicallyoccursduringdownstreamprocessingstepssuchasheattreating,pickling,andcleaning.TheLECOONH836isasimultaneousoxygen,nitrogen,andhydrogendeterminatorthatutilizesanelectrodefurnace,inertcarriergas,andbothinfraredandthermalconductivitydetectiontomeettheanalyticalneedsoftherefractorymetalindustry.ThisapplicationnotewaswrittenspecificallyforusewiththeLECOONH836seriesdeterminator.上海禹重實業(yè)有限公司致力于提供分析儀,有想法的可以來電咨詢!靜安區(qū)氧氮氫分析儀咨詢報價
companyprofileShanghaiUzongIndustrialCo.,Ltd.(hereinafterreferredtoasUZONGLAB®)isahigh-techcompanythatprovidesintegratedsolutionsforintelligentlaboratories,mainlyservingtheChinesemarketandcountriesalongthe“BeltandRoad”.IthasthreebusinessdivisionsandoneThetechnologycenter,namelytheinstrumentbusinessdepartment,consumablesbusinessdepartment,projectdevelopmentdepartment,andZhongyuLianheTechnologyCenter.InadditiontotheShanghaiheadquarters,wehaveestablishedbranchesinBeijing,Shenyang,Shijiazhuang,Taiyuan,Qingdao,Guangzhou,ChengduandUrumqi.Toprovidecustomerswithmoreprofessional,saferandmoreconvenientproductsandservicesisoursolegoal.淮北原裝分析儀咨詢報價上海禹重實業(yè)有限公司是一家專業(yè)提供分析儀的公司,有需求可以來電咨詢!
SamplePreparationTypically,titaniumandzirconiumsamplesarechemicallyetchedtoremovesurfacecontaminationwhenoxygenandnitrogenaredetermined.However,etchingcanintroducehydrogenintothesample.ASTMmethodE1409"DeterminationofOxygenandNitrogeninTitaniumandTitaniumAlloysbytheInertGasFusionTechnique",asupdatedin1996,permitseitheretchingorabrading(filing)ofthetestspecimen.ASTME1447"DeterminationofHydrogeninTitaniumandTitaniumAlloysbytheInertGasFusionThermalConductivity/InfraredDetectionMethod"permitssurfacepreparationbyabrading(ifnecessarytoremovecontamination).DifferencesinsamplepreparationpresentsomewhatofadilemmaregardingsimultaneousdeterminationofO,N,andHintitanium.However,abradingsampleswithafiletoremovesurfacecontaminationwillyieldaccurateO,N,andHresults.TheONH836utilizesahigh-powerelectrodefurnacetoquicklyandefficientlyreleasethetargetgasesfromwithinthesample,whichallowsforaveryrapidsimultaneousdeterminationofoxygen,nitrogen,andhydrogen.
Instrumentcalibration/driftcorrection.a.Loginaminimumof3Standardreplicates.b.Weigha~1.000gramofacalibration/driftstandard,enterthemassandstandardidentificationintoappropriatereplicatefields.c.PresstheAnalyzebuttonontheinstrumentscreen.Afterashortdelay,theloadingheadslide-blockwillopen.d.Placethecalibration/driftstandardintotheopenportatthetopoftheloadinghead.e.PresstheAnalyzebuttonontheinstrumentscreenagain,theloadingheadslide-blockwillcloseandthelowerelectrodewillopen.上海禹重實業(yè)有限公司為您提供分析儀,歡迎新老客戶來電!
氧氮氫分析儀的原理:分析樣品在惰性氣流存在下于石墨坩堝中加熱熔融,其中脈沖爐溫度可自由設(shè)定,并通過一個非接觸式的光學(xué)溫度傳感器進行實時監(jiān)控,用于實現(xiàn)樣品的完全分解,反應(yīng)所生成的COH2和N2被帶入到具有高穩(wěn)定性和靈敏度的檢測系統(tǒng)進行檢測。對于CO的檢測采用的是非色散性紅外檢測器,對于N2和H2的檢測則采用熱導(dǎo)檢測器。氧氮氫分析儀的特點:快速準確分析,自動化操作;精密氣體校準;CO紅外檢測器,高分辨率和重現(xiàn)性的N、H熱導(dǎo)池檢測器;同一臺儀器實現(xiàn)熔融提取和熱提??;熱提取分析時間可調(diào);可自由選擇溫度高達2500°C;光學(xué)溫度計溫度測定和控制;所有檢測器自動調(diào)零/自動水平控制(ALC);數(shù)據(jù)評估的自動優(yōu)化選擇范圍;爐自動清潔和坩堝自動進樣(可選);外設(shè)電腦進行操作和控制;樣品信息保存;所有樣品數(shù)據(jù)可追蹤查詢;通過FTP或本地局域網(wǎng)進行數(shù)據(jù)傳輸;ON,H分析輕松切換。上海禹重實業(yè)有限公司致力于提供分析儀,歡迎您的來電!臺州力可LECO分析儀
分析儀,就選上海禹重實業(yè)有限公司,歡迎客戶來電!靜安區(qū)氧氮氫分析儀咨詢報價
Procedure-SolidSamplesDeterminetheinstrumentblank.Repeatsteps2bthrough2gaminimumofthreetimes.Settheblankfollowingtheprocedureoutlinedintheoperatorsinstructionmanual.Instrumentcalibration/driftcorrection.Loginaminimumof3Standardreplicates.Weighapproximately***gramsofacalibration/driftstandard,enterthemassandstandardidentificationintoappropriatereplicatefields.Note:LECOReferenceMateria***onotrequirepreparation.Seepreparationstatementonthereferencematerialcertificate.靜安區(qū)氧氮氫分析儀咨詢報價
上海禹重實業(yè)有限公司是一家有著雄厚實力背景、信譽可靠、勵精圖治、展望未來、有夢想有目標,有組織有體系的公司,堅持于帶領(lǐng)員工在未來的道路上大放光明,攜手共畫藍圖,在上海市等地區(qū)的儀器儀表行業(yè)中積累了大批忠誠的客戶粉絲源,也收獲了良好的用戶口碑,為公司的發(fā)展奠定的良好的行業(yè)基礎(chǔ),也希望未來公司能成為*****,努力為行業(yè)領(lǐng)域的發(fā)展奉獻出自己的一份力量,我們相信精益求精的工作態(tài)度和不斷的完善創(chuàng)新理念以及自強不息,斗志昂揚的的企業(yè)精神將**上海禹重實業(yè)供應(yīng)和您一起攜手步入輝煌,共創(chuàng)佳績,一直以來,公司貫徹執(zhí)行科學(xué)管理、創(chuàng)新發(fā)展、誠實守信的方針,員工精誠努力,協(xié)同奮取,以品質(zhì)、服務(wù)來贏得市場,我們一直在路上!